Mass Spectrometry in Polymer Chemistry
(Sprache: Englisch)
Written by the world s most proficient experts, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric techniques, enabling both newcomers and experienced researchers to choose the appropriate methods and instrumentation.
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Produktinformationen zu „Mass Spectrometry in Polymer Chemistry “
Written by the world s most proficient experts, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric techniques, enabling both newcomers and experienced researchers to choose the appropriate methods and instrumentation.
Klappentext zu „Mass Spectrometry in Polymer Chemistry “
Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods.Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book.As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.
Mass spectrometry is a powerful analytical tool for the determination of the chemical composition, structure and molecular weight of organic compounds. Already widely used in the life sciences, mass spectrometry has become an indispensable characterization method in polymer chemistry - in basic research as well as in industrial laboratory settings. Mass spectrometry can be integrated seamlessly with other analytical techniques such as liquid chromatography. Its sensitivity and specifity make it a versatile means for the qualitative and quantitative elucidation of polymer composition, functionality and reaction mechanisms.
Combining an up-to-date insight into mass spectrometry polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass spectrometric methods. The book provides the state-of-the-art knowledge on mass spectrometry for the synthetically working chemist, enabling the researcher to choose the appropriate methods and instrumentations - and to assess their respective strenghths and limitations - for the characterization of polymer compounds.
Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering important technologies and applications such as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separations, secondary ion mass spectrometry and automated data processing.
This book is a must-have for all Polymer and Analytical Chemists, Materials Scientists, Spectroscopists, and Chemists in Industry. an up-to-date insight into mass spectrometry polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass spectrometric methods. The book provides the state-of-the-art knowledge on mass spectrometry for the synthetically working chemist, enabling the researcher
Combining an up-to-date insight into mass spectrometry polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass spectrometric methods. The book provides the state-of-the-art knowledge on mass spectrometry for the synthetically working chemist, enabling the researcher to choose the appropriate methods and instrumentations - and to assess their respective strenghths and limitations - for the characterization of polymer compounds.
Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering important technologies and applications such as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separations, secondary ion mass spectrometry and automated data processing.
This book is a must-have for all Polymer and Analytical Chemists, Materials Scientists, Spectroscopists, and Chemists in Industry. an up-to-date insight into mass spectrometry polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass spectrometric methods. The book provides the state-of-the-art knowledge on mass spectrometry for the synthetically working chemist, enabling the researcher
Inhaltsverzeichnis zu „Mass Spectrometry in Polymer Chemistry “
IntroductionMASS ANALYSISIntroductionMeasures of PerformanceInstrumentationInstrumentation in Tandem and Multiple-Stage Mass SpectrometryConclusions and OutlookIONIZATION TECHNIQUES FOR POLMYER MASS SPECTROMETRYIntroductionSmall Molecule Ionization EraMacromass Era of IonizationModern Era of Ionization TechniquesConclusionsTANDEM MASS SPECTROMETRY ANALYSIS OF POLYMER STRUCTURES AND ARCHITECTURESIntroductionActivation MethodsInstrumentationStructural Information from MS2 StudiesSummary and OutlookMATRIX-ASSISTED INLET IONIZATION AND SOLVENT-FREE GAS-PHASE SEPARATION USING ION MOBILITY SPECTROMETRY FOR IMAGING AND ELECTRON TRANSFER DISSOCIATION MASS SPECTROMETRY OF POLYMERSOverviewIntroductionNew Sample Introduction TechnologiesFragmentation by ETD and CIDSurface Analyses by Imaging MSFuture OutlookPOLYMER MALDI SAMPLE PREPARATIONIntroductionRoles of the MatrixChoice of MatrixChoice of the SolventBasic Solvent-Based Sample Preparation RecipeDeposition MethodsSolvent-Free Sample PreparationThe Vortex MethodMatrix-to-Analyte RatioSalt-to-Analyte RatioChromatography as Sample PreparationProblems in MALDI Sample PreparationPredicting MALDI Sample PreparationConclusionsSURFACE ANALYSIS AND IMAGING TECHNIQUESImaging Mass SpectrometrySecondary Ion Mass SpectrometryMatrix-Assisted Laser Desorption Ionization (MALDI)Other Surface Mass Spectrometry MethodsOutlookHYPHENATED TECHNIQUESIntroductionPolymer Separation TechniquesPrinciples of Coupling: Transfer DevicesExamplesConclusionsAUTOMATED DATA PROCESSING AND QUANTIFICATION IN POLMYER MASS SPECTROMETRYIntroductionFile and Data FormatsOptimization of Ionization ConditionsAutomated Spectral Analysis and Data Reduction in MSCopolymer AnalysisData Interpretation in MS/MSQuantitative MS and the Determination of MMDs by MSConclusions and OutlookCOMPREHENSIVE COPOLYMER CHARACTERIZATIONIntroductionScopeReviewsSoft Ionization TechniquesSeparation Prior MSTandem MS (MS/MS)Quantitative MSCopolymers for Biological or (Bio)medical
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ApplicationSoftware DevelopmentSummary and OutlookELUCIDATION OF REACTION MECHANISMS: CONVENTIONAL RADICAL POLYMERIZATIONIntroductionBasic Principles and General ConsiderationsInitiationPropagationTerminationChain TransferEmulsion PolymerizationConclusionELUCIDATION OF REACTION MECHANISMS AND POLYMER STRUCTURE: LIVING/CONTROLLED RADICAL POLYMERIZATIONProtocols Based on a Persistent Radical Effect (NMP, ATRP, and Related)Protocols Based on Degenerative Chain Transfer (RAFT, MADIX)Protocols Based on CCTNovel Protocols and Minor ProtocolsConclusionsELUCIDATON OF REACTION MECHANISMS: OTHER POLYMERIZATION MECHANISMSIntroductionRing-Opening Polymerization Mechanisms of Cyclic EthersRing-Opening Polymerization Mechanisms of Cyclic Ethers and CarbonatesRing-Opening Metathesis PolymerizationMechanisms of Step-Growth PolymerizationConcluding RemarksPOLYMER DEGRADATIONIntroductionThermal and Thermo-Oxidative DegradationPhotolysis and PhotooxidationBiodegradationOther Degradation ProcessesConclusionsOUTLOOK
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Autoren-Porträt
Christopher Barner-Kowollik is currently Full Professor of Preparative Macromolecular Chemistry at the Karlsruhe Institute of Technology (KIT), Germany. He has published more than 200 peer-reviewed research papers and nine book chapters. He serves or has served as a member of six editorial boards of leading peer-reviewed journals and edited the "Handbook of RAFT Polymerization" (2008, Wiley-VCH). Awards he has received for his research include the Edgeworth-David Medal of the Royal Society of Australia and the Rennie Medal of the Royal Australian Chemical Institute.Till Gründling completed his PhD at the University of New South Wales under the supervision of Christopher Barner-Kowollik and Brynn Hibbert. He is currently postdoctoral researcher in the Preparative Macromolecular Chemistry group at the Karlsruhe Institute of Technology (KIT). Till Gründling has published ten peer-reviewed research papers and has presented his work at international conferences. His research involves the application of liquid chromatography-mass spectrometry (LC-MS) and the development of novel quantitative methods in LC-MS.nstitute of Technology (KIT), Germany. He has published more than 200 peer-reviewed research papers and nine book chapters. He serves or has served as a member of six editorial boards of leading peer-reviewed journals and edited the "Handbook of RAFT Polymerization" (2008, Wiley-VCH). Awards he has received for his research include the Edgeworth-David Medal of the Royal Society of Australia and the Rennie Medal of the Royal Australian Chemical Institute.
Till Gründling completed his PhD at the University of New South Wales under the supervision of Christopher Barner-Kowollik and Brynn Hibbert. He is currently postdoctoral researcher in the Preparative Macromolecular Chemistry group at the Karlsruhe Institute of Technology (KIT). Till Gründling has published ten peer-reviewed research papers and has presented his work at international conferences. His research
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involves the applicat
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Bibliographische Angaben
- 2011, XVI, 484 Seiten, 30 farbige Abbildungen, 60 Schwarz-Weiß-Abbildungen, Maße: 17,7 x 25 cm, Gebunden, Englisch
- Herausgegeben: Christopher Barner-Kowollik, Till Gruendling, Jana Falkenhagen, Steffen Weidner
- Verlag: Wiley-VCH
- ISBN-10: 3527329242
- ISBN-13: 9783527329243
- Erscheinungsdatum: 12.12.2011
Sprache:
Englisch
Rezension zu „Mass Spectrometry in Polymer Chemistry “
"There is much to laud the editors for the production of this work ... As the editors have so clearly achieved their stated goals, it is easy to be enthusiastic about this volume and to recommend it to anyone interested in polymer chemistry or mass spectrometry as a needed resource." ( American Society for Mass Spectrometry , 11 August 2012)
Pressezitat
"Taken as a whole, this book gives an excellent overview of the current state of mass spectrometry being applied to modern, complex polymer systems." ( Chromatographia , 1 August 2013)"There is much to laud the editors for the production of this work . . . As the editors have so clearly achieved their stated goals, it is easy to be enthusiastic about this volume and to recommend it to anyone interested in polymer chemistry or mass spectrometry as a needed resource." ( American Society for Mass Spectrometry , 11 August 2012)
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