Practical Microwave Synthesis for Organic Chemists
Stategies, Instruments, and Protocols
(Sprache: Englisch)
With the novice user in mind, this beginner s guide explains the basics behind microwave technology, evaluates available instruments and reaction modes, and provides practical hints for every eventuality. Includes 27 detailed protocols for often-used...
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Klappentext zu „Practical Microwave Synthesis for Organic Chemists “
With the novice user in mind, this beginner s guide explains the basics behind microwave technology, evaluates available instruments and reaction modes, and provides practical hints for every eventuality. Includes 27 detailed protocols for often-used reactions.From the contents:
1 Microwave Synthesis - An Introduction
2 Microwave Theory
3 Equipment Review
4 Microwave Processing Techniques
5 Starting With Microwave Chemistry
6 Experimental Protocols
6.1 General Small-Scale Sealed-Vessel Microwave Processing
6.2 Reaction Optimization
6.3 Library Generation
6.4 Reaction Scale-Up
6.5 Special Processing Techniques
Inhaltsverzeichnis zu „Practical Microwave Synthesis for Organic Chemists “
Introduction to Microwave-assisted SynthesisBasic Principles of Microwave Chemistry
- radiation, dielectric heating, microwave effects
Microwave Reactors for Organic Synthesis
- single- and multimode cavities, overview of commercially available instruments
Getting Started with Microwaves
- how and when to use microwaves, practical tips, safety aspects
General Methods
- open/closed vessels, parallel processing
Practical Examples of Microwave-assisted Reactions
- contains detailed descriptions of more than 30 experiments
- includes real data obtained with different microwave reactors
Outlook and Conclusion
Bibliographische Angaben
- Autoren: C. Oliver Kappe , Doris Dallinger , Shaun S. Murphree
- 2008, X, 300 Seiten, Maße: 17,5 x 25 cm, Gebunden, Englisch
- Verlag: Wiley-VCH
- ISBN-10: 3527320970
- ISBN-13: 9783527320974
- Erscheinungsdatum: 06.01.2009
Sprache:
Englisch
Rezension zu „Practical Microwave Synthesis for Organic Chemists “
"The authors present a good over view of the tools and methods for micro wave-assisted organic synthesis (MOAS)." ( The C atalyst , 1 February 2012) "The authors have produced a gem of a book, and in an area where coherent practical training is lacking, this book is a welcome addition." ( Development and Change July, 2009) "I read this book with pleasure... I am sure that this excellent guide will become the standard reference work in the field and clearly is a 'must have' for anybody getting started with microwave-assisted organic chemistry." ( Angewandte Chemie International Edition , April 2009)
Pressezitat
"The authors present a good over view of the tools and methods for micro wave-assisted organic synthesis (MOAS)." ( The C atalyst , 1 February 2012)"The authors have produced a gem of a book, and in an area where coherent practical training is lacking, this book is a welcome addition." ( Development and Change July, 2009)
"I read this book with pleasure.... I am sure that this excellent guide will become the standard reference work in the field and clearly is a must have for anybody getting started with microwave-assisted organic chemistry." ( Angewandte Chemie International Edition , April 2009)
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