A Microscale Approach to Organic Laboratory Techniques, International Edition
(Sprache: Englisch)
From biofuels, green chemistry, and nanotechnology, this proven laboratory textbook provides the up-to-date coverage students need in their coursework and future careers. The book's experiments, all designed to utilize microscale glassware and equipment,...
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Klappentext zu „A Microscale Approach to Organic Laboratory Techniques, International Edition “
From biofuels, green chemistry, and nanotechnology, this proven laboratory textbook provides the up-to-date coverage students need in their coursework and future careers. The book's experiments, all designed to utilize microscale glassware and equipment, cover traditional organic reactions and syntheses, the isolation of natural products, and molecular modeling and include project-based experiments and experiments that have a biological or health science focus. Updated throughout with new and revised experiments, new and revised essays, and revised and expanded techniques, the Fifth Edition is organized based on essays and topics of current interest.
Inhaltsverzeichnis zu „A Microscale Approach to Organic Laboratory Techniques, International Edition “
PART I: INTRODUCTION TO BASIC LABORATORY TECHNIQUES.Experiment 1: Introduction to Microscale Laboratory.
Experiment 2: Solubility.
Experiment 3: Crystallization.
Experiment 4: Extraction.
Experiment 5: A Separation and Purification Scheme.
Experiment 6: Chromatography.
Experiment 7: Simple and Fractional Distillation.
Experiment 8: Infrared Spectroscopy and Boiling Point Determination.
ESSAY: Aspirin.
Experiment 9: Acetylsalicylic Acid.
ESSAY: Analgesics.
Experiment 10: Isolation of the Active Ingredient in an Analgesic Drug.Experiment 11: Acetaminophen.
ESSAY: Identification of Drugs.
Experiment 12: TLC Analysis of Analgesic Drugs.
ESSAY: Caffeine.
Experiment 13: Isolation of Caffeine.
ESSAY: Esters -- Flavors and Fragrances.
Experiment 14: Isopentyl Acetate (Banana Oil).
ESSAY: Terpenes and Phenylpropanoids.
Experiment 15: Essential Oils: Extraction of Oil of Cloves by Steam Distillation.
Essay: Stereochemical Theory of Odor.
Experiment 16: Spearmint and Caraway Oil: (+)- and (-)- Carvones.
Essay:The Chemistry of Vision.
Experiment 17: Isolation of Chlorophyll and Carotenoid Pigments from Spinach.
Essay: Ethanol and Fermentation Chemistry.
Experiment 18 Ethanol from Sucrose.
PART II: INTRODUCTION TO MOLECULAR MODELING.
ESSAY: Molecular Modeling and Molecular Mechanics.
Experiment 19: An Introduction to Molecular Modeling.
ESSAY: Computational Chemistry -- Ab initio and Semiempirical Methods.
Experiment 20: Computational Chemistry.
PART III: PROPERTIES AND REACTIONS OF ORGANIC COMPOUNDS.
Experiment 21: Reactivities of Some Alkyl Halides.
Experiment 22: Nucleophilic Substitution Reactions: Competing Nucleophiles.
Experiment 23: Synthesis of n-Butyl Bromide and t-Pentyl Chloride.
Experiment 24: 4-Methylcyclohexene.
ESSAY: Fats and Oils.
Experiment 25: Methyl Stearate from Methyl Oleate.
ESSAY: Petroleum and Fossil Fuels.
Experiment 26: Gas Chromatographic Analysis of Gasolines.
ESSAY: Biofuels.
Experiment 27:
... mehr
Biodiesel.
ESSAY: Green Chemistry.
Experiment 28: Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination Using a Chiral Shift Reagent.
Experiment 29: Nitration of Aromatic Compounds Using a Recyclable Catalyst.
Experiment 30: Resolution of (?????Phenylethylamine and Determination of Optical Purity.
Experiment 31: An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol.
Experiment 32: Multi-Step Reaction Sequences: The Conversion of Benzaldehyde to Benzilic Acid.
Experiment 33: Triphenylmethanol and Benzoic Acid.
Experiment 34: Sonogashira Coupling of Iodosubstituted Aromatic Compounds with Alkynes Using a Palladium Catalyst.
Experiment 35: Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butanediol to Prepare a Natural Product.
Experiment 36: Aqueous-based Organozinc Reactions.
Experiment 37: The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones).
Experiment 38: Preparation of an ???-Unsaturated Ketone via Michael and Aldol Condensation Reactions.
Experiment 39: The Wittig Reaction: Preparation of 1,4-Diphenyl-1,3-butadiene.
Experiment 40: Relative Reactivities of Several Aromatic Compounds.
Experiment 41: Nitration of Methyl Benzoate.
ESSAY: Local Anesthetics.
Experiment 42: Benzocaine.
Experiment 43: Methyl Salicylate (Oil of Wintergreen).
ESSAY: Pheromones: Insect Attractants and Repellents.
Experiment 44: N,N-Diethyl-m-toluamide: The Insect Repellent OFF."
ESSAY:Sulfa Drugs.
Experiment 45: Sulfa Drugs: Preparation of Sulfanilamide.
Essay: Polymers and Plastics.
Experiment 46: Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene.
Essay: Diels-Alder Reactions and Insecticides.
Experiment 47: The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride.
Experiment 48: Diels-Alder Reaction with Anthracene-9-methanol.
Experiment 49: Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone.
ESSAY:Fireflies and Photochemistry.
Experiment 50: Luminol.
ESSAY: The
ESSAY: Green Chemistry.
Experiment 28: Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination Using a Chiral Shift Reagent.
Experiment 29: Nitration of Aromatic Compounds Using a Recyclable Catalyst.
Experiment 30: Resolution of (?????Phenylethylamine and Determination of Optical Purity.
Experiment 31: An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol.
Experiment 32: Multi-Step Reaction Sequences: The Conversion of Benzaldehyde to Benzilic Acid.
Experiment 33: Triphenylmethanol and Benzoic Acid.
Experiment 34: Sonogashira Coupling of Iodosubstituted Aromatic Compounds with Alkynes Using a Palladium Catalyst.
Experiment 35: Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butanediol to Prepare a Natural Product.
Experiment 36: Aqueous-based Organozinc Reactions.
Experiment 37: The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones).
Experiment 38: Preparation of an ???-Unsaturated Ketone via Michael and Aldol Condensation Reactions.
Experiment 39: The Wittig Reaction: Preparation of 1,4-Diphenyl-1,3-butadiene.
Experiment 40: Relative Reactivities of Several Aromatic Compounds.
Experiment 41: Nitration of Methyl Benzoate.
ESSAY: Local Anesthetics.
Experiment 42: Benzocaine.
Experiment 43: Methyl Salicylate (Oil of Wintergreen).
ESSAY: Pheromones: Insect Attractants and Repellents.
Experiment 44: N,N-Diethyl-m-toluamide: The Insect Repellent OFF."
ESSAY:Sulfa Drugs.
Experiment 45: Sulfa Drugs: Preparation of Sulfanilamide.
Essay: Polymers and Plastics.
Experiment 46: Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene.
Essay: Diels-Alder Reactions and Insecticides.
Experiment 47: The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride.
Experiment 48: Diels-Alder Reaction with Anthracene-9-methanol.
Experiment 49: Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone.
ESSAY:Fireflies and Photochemistry.
Experiment 50: Luminol.
ESSAY: The
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Bibliographische Angaben
- Autoren: Donald L. Pavia , Gary M. Lampman , George S. Kriz
- 2012, 5th ed., 1040 Seiten, Maße: 27,6 cm, Kartoniert (TB), Englisch
- With Donald L. Pavia, Gary M. Lampman, George S. Kriz, Randall G. Engel
- Verlag: Cengage Learning EMEA
- ISBN-10: 1133107419
- ISBN-13: 9781133107415
Sprache:
Englisch
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