Inorganic Synthesis.Vol.35
(Sprache: Englisch)
The Inorganic Syntheses series provides all users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely compounds.
* Includes complete, up-to-date procedures involving important inorganic substances
*...
* Includes complete, up-to-date procedures involving important inorganic substances
*...
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Klappentext zu „Inorganic Synthesis.Vol.35 “
The Inorganic Syntheses series provides all users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely compounds.* Includes complete, up-to-date procedures involving important inorganic substances
* Contains subject, contributor, and formula indexes
Inhaltsverzeichnis zu „Inorganic Synthesis.Vol.35 “
Preface.Contributors.
Dedication.
Notice to Contributors and Checkers.
Toxic Substances and Laboratory Hazards.
Chapter One COMPLEXES OF BULKY ß-DIKETIMINATE LIGANDS.
1. Introduction.
2. ß-Diketiminate Precursors HL¯Me,Me3 and TlL¯Me,Me3 (L¯Me,Me3 = 2,4-Bis-(Mesitylimido)Pentyl).
3. ß-Diketiminate Precursors L¯Me,iPr2H, [¯LMe,iPr2Li]x, and [L¯tBu,iPr2K]x (L¯Me,iPr2 = 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl; L¯tBu,iPr2 = 2,2,6,6-
Tetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido)Heptyl).
4. ß-Diketiminate Precursors L¯tBu,iPr2H and L¯tBu,iPr2Li(THF) (L¯tBu,iPr2=2,2,6,6-Tetramethyl-3,5- Bis-(2,6-Diisopropylphenylimido)Heptyl).
5. Scandium Trichloride Tris(Tetrahydrofuran) and ß-Diketiminate-Supported Scandium Chloride Complexes.
6. ß-Diketiminate-Supported Titanium and Vanadium Dichloride Complexes.
7. ß-Diketiminate-Supported Vanadium and Chromium Chloride Complexes.
8. ß-Diketiminate-Supported Manganese and Zinc Complexes.
9. Iron 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride (L¯Me,iPr2FeCl).
10. Iron 2,2,6,6-Tetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido)Heptyl Chloride (L¯tBu,iPr2FeCl).
11. Cobalt 2,2,6,6-Tetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido) Heptyl Chloride (L¯tBu,iPr2CoCl).
12. ß-Diketiminate-Supported Nickel(II) and Nickel(I) Complexes of L¯Me,Me3 (L¯Me,Me3 = 2,4-Bis-(Mesitylimido)Pentyl).
13. Nickel 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride Dimer, [L¯Me,iPr2Ni(µ-Cl)]2.
14. Bis[Copper 2,4-Bis-(2,4,6-Trimethylphenylimido)Pentyl] Toluene, (L¯Me,Me3Cu)2(µ-n²:n²-C7H8).
15. Copper 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride (L¯Me,iPr2CuCl).
Chapter Two BORON CLUSTER COMPOUNDS.
16. Salts of Dodecamethylcarba-closo-Dodecaborate(--) Anion, CB11Me12, and the Radical Dodecamethylcarba-closo-Dodecaboranyl, CB11Me12.
17.
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Cesium Dodecahydroxy-closo-Dodecaborate, Cs2[B12(OH)12].
Chapter Three COORDINATION COMPOUNDS.
18. Pentaaquanitrosylchromium Sulfate.
19. The Tetradentate Bispidine Ligand Dimethyl-(3,7-Dimethyl-9-oxo-2,4-bis(2-pyridyl)-3,7-Diazabicyclo[3.3.1]nonane)-1, 5-dicarboxylate and Its Copper(ll) Complex.
20. Tris(2-Picolinyl)Methane and Its Copper(I) Complex.
Chapter Four CARBENE LIGANDS AND COMPLEXES.
21. 1,3-Dialkyl-Imidazole-2-Ylidenes.
22. A Chelating Rhodium N-Heterocyclic Carbene Complex by Transmetallation from a Silver-NHC Intermediate.
23. Rhodium and Iridium N-Heterocyclic Carbene Complexes from Imidazolium Carboxylates.
Chapter Five FUNCTIONAL LIGANDS AND COMPLEXES.
24. N-tert-Butyl ortho-Aminophenol, ortho-Iminoquinone, and a Zirconium(IV) bis(Aminophenolate) Complex.
25. Synthesis of the Water-Soluble Bidentate (P, N) Ligand PTN(Me) (PTN(Me) = 7-Phospha-3-methyl-1,3,5-triazabicyclo[3.3.1]nonane).
26. Synthesis of Metal-Organic Frameworks: MOF-5 and MOF-177.
Chapter Six ORGANOMETALLIC REAGENTS.
27. Tricarbonyl 1,3,5-Trimethyl-1,3,5-Triazacyclohexane Complexes of Chromium(0), Molybdenum(0), and Tungsten(0) [M(CO)3(Me3TACH) (M = Cr, Mo, W)].
28. Manganese Tricarbonyl Transfer (MTT) Agents.
29. Bis(1,5-Cyclooctadiene)Nickel(0).
30. Sodium (n¯5-Cyclopentadienyl)Tris(Dimethylphosphito-P) Cobaltate(III), Na[(C5H5)Co{P(O)(OMe)2}3].
Chapter Seven BIO-INSPIRED IRON AND NICKEL COMPLEXES.
31. Iron-Cyanocarbonyl Complexes [PPN][Fe(CO)4(CN)] and [PPN][FeBr(CO)3(CN)2].
32. Nickel Complexes of Bis(Diethylphosphinomethyl) Methylamine.
33. Monomeric Iron(II) Complexes Having Two Sterically Hindered Arylthiolates.
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Chapter Three COORDINATION COMPOUNDS.
18. Pentaaquanitrosylchromium Sulfate.
19. The Tetradentate Bispidine Ligand Dimethyl-(3,7-Dimethyl-9-oxo-2,4-bis(2-pyridyl)-3,7-Diazabicyclo[3.3.1]nonane)-1, 5-dicarboxylate and Its Copper(ll) Complex.
20. Tris(2-Picolinyl)Methane and Its Copper(I) Complex.
Chapter Four CARBENE LIGANDS AND COMPLEXES.
21. 1,3-Dialkyl-Imidazole-2-Ylidenes.
22. A Chelating Rhodium N-Heterocyclic Carbene Complex by Transmetallation from a Silver-NHC Intermediate.
23. Rhodium and Iridium N-Heterocyclic Carbene Complexes from Imidazolium Carboxylates.
Chapter Five FUNCTIONAL LIGANDS AND COMPLEXES.
24. N-tert-Butyl ortho-Aminophenol, ortho-Iminoquinone, and a Zirconium(IV) bis(Aminophenolate) Complex.
25. Synthesis of the Water-Soluble Bidentate (P, N) Ligand PTN(Me) (PTN(Me) = 7-Phospha-3-methyl-1,3,5-triazabicyclo[3.3.1]nonane).
26. Synthesis of Metal-Organic Frameworks: MOF-5 and MOF-177.
Chapter Six ORGANOMETALLIC REAGENTS.
27. Tricarbonyl 1,3,5-Trimethyl-1,3,5-Triazacyclohexane Complexes of Chromium(0), Molybdenum(0), and Tungsten(0) [M(CO)3(Me3TACH) (M = Cr, Mo, W)].
28. Manganese Tricarbonyl Transfer (MTT) Agents.
29. Bis(1,5-Cyclooctadiene)Nickel(0).
30. Sodium (n¯5-Cyclopentadienyl)Tris(Dimethylphosphito-P) Cobaltate(III), Na[(C5H5)Co{P(O)(OMe)2}3].
Chapter Seven BIO-INSPIRED IRON AND NICKEL COMPLEXES.
31. Iron-Cyanocarbonyl Complexes [PPN][Fe(CO)4(CN)] and [PPN][FeBr(CO)3(CN)2].
32. Nickel Complexes of Bis(Diethylphosphinomethyl) Methylamine.
33. Monomeric Iron(II) Complexes Having Two Sterically Hindered Arylthiolates.
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Bibliographische Angaben
- Autoren: Al Sattelberger , Bodie E. Douglas
- 2010, 1. Auflage, 300 Seiten, Maße: 23,3 cm, Gebunden, Englisch
- Herausgegeben: Thomas Rauchfuss
- Verlag: Wiley & Sons
- ISBN-10: 0471682551
- ISBN-13: 9780471682554
- Erscheinungsdatum: 13.12.2010
Sprache:
Englisch
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