Understanding NMR Spectroscopy
(Sprache: Englisch)
Understanding NMR SpectroscopyJames Keeler Department of Chemistry, University of Cambridge, UKThis text discusses the high-resolution NMR of liquid samples and concentrates exclusively on spin-half nuclei (mainly 1H and 13C). It is aimed at people who are...
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Understanding NMR Spectroscopy
James Keeler Department of Chemistry, University of Cambridge, UK
This text discusses the high-resolution NMR of liquid samples and concentrates exclusively on spin-half nuclei (mainly 1H and 13C). It is aimed at people who are familiar with the use of routine NMR for structure determination and who wish to deepen their understanding of just exactly how NMR experiments work. It demonstrates that in NMR it is possible, quite literally on the back of an envelope, to make exact predictions of the outcome of quite sophisticated experiments. The experiments chosen are likely to be encountered in the routine NMR of small to medium-sized molecules, but are also applicable to the study of large biomolecules, such as proteins and nucleic acids.
The book starts off at a gentle pace, working through some more-or-less familiar ideas, and then elaborating these as the book progresses. Each chapter ends with exercises which are designed to assist in the understanding of the ideas presented and to grasp the underlying ideas.
Klappentext zu „Understanding NMR Spectroscopy “
Understanding NMR SpectroscopyJames Keeler Department of Chemistry, University of Cambridge, UKThis text discusses the high-resolution NMR of liquid samples and concentrates exclusively on spin-half nuclei (mainly 1H and 13C). It is aimed at people who are familiar with the use of routine NMR for structure determination and who wish to deepen their understanding of just exactly how NMR experiments work. It demonstrates that in NMR it is possible, quite literally on the back of an envelope, to make exact predictions of the outcome of quite sophisticated experiments. The experiments chosen are likely to be encountered in the routine NMR of small to medium-sized molecules, but are also applicable to the study of large biomolecules, such as proteins and nucleic acids.The book starts off at a gentle pace, working through some more-or-less familiar ideas, and then elaborating these as the book progresses. Each chapter ends with exercises which are designed to assist in the understanding of the ideas presented and to grasp the underlying ideas.
Inhaltsverzeichnis zu „Understanding NMR Spectroscopy “
1. What this book is about and who should read it.2. Setting the scene.
3. Energy levels and NMR spectra.
4. The vector model.
5. Fourier transformation and data processing.
6. The quantum mechanics of one spin.
7. Product operators.
8. Two-dimensional NMR.
9. Relaxation and the NOE.
10. Advanced topics in tow-dimensional NMR.
11. Coherence selection: phase cycling and field gradient pulses.
12. How the spectrometer works.
Appendix: Some mathematical topics.
Index.
Autoren-Porträt von James Keeler
Dr James Keeler is responsible for undergraduate studies in chemistry and related subjects at the University of Cambridge. He is an active research in the development of new methodologies in NMR and is Editor-in-Chief of Magnetic Resonance in Chemistry.
Bibliographische Angaben
- Autor: James Keeler
- 2005, XV, 459 Seiten, mit Schwarz-Weiß-Abbildungen, Maße: 19 x 2,9 cm, Kartoniert (TB), Englisch
- Verlag: Wiley & Sons
- ISBN-10: 0470017872
- ISBN-13: 9780470017876
Sprache:
Englisch
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