Flash Chemistry
Fast Organic Synthesis in Microsystems
(Sprache: Englisch)
Flash chemistry is a new concept which offers an integrated scheme for fast, controlled organic synthesis. The first book to describe this exciting new technique, Flash Chemistry brings together research in reactive intermediates and microreactors into an...
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Produktinformationen zu „Flash Chemistry “
Flash chemistry is a new concept which offers an integrated scheme for fast, controlled organic synthesis. The first book to describe this exciting new technique, Flash Chemistry brings together research in reactive intermediates and microreactors into an integrated scheme for fast, controlled organic synthesis.
Klappentext zu „Flash Chemistry “
Have you ever wished you could speed up your organic syntheses without losing control of the reaction? Flash Chemistry is a new concept which offers an integrated scheme for fast, controlled organic synthesis. It brings together the generation of highly reactive species and their reactions in microsystems to enable highly controlled organic syntheses on a preparative scale in timescales of a few seconds or less.Flash Chemistry - Fast Chemical Reactions in Microsystems is the first dedicated book to describe this exciting new technique, and is an essential introduction for anyone working in organic synthesis, process chemistry, chemical engineering and physical organic chemistry concerned with fundamental aspects of chemical reactions and synthesis and the production of organic compounds.
Have you ever wished you could speed up your organic syntheses without losing control of the reaction? Flash Chemistry is a new concept which offers an integrated scheme for fast, controlled organic synthesis. It brings together the generation of highly reactive species and their reactions in microsystems to enable highly controlled organic syntheses on a preparative scale in timescales of a few seconds or less.
Flash Chemistry - Fast Chemical Reactions in Microsystems is the first dedicated book to describe this exciting new technique, and is an essential introduction for anyone working in organic synthesis, process chemistry, chemical engineering and physical organic chemistry concerned with fundamental aspects of chemical reactions and synthesis and the production of organic compounds.
Flash Chemistry - Fast Chemical Reactions in Microsystems is the first dedicated book to describe this exciting new technique, and is an essential introduction for anyone working in organic synthesis, process chemistry, chemical engineering and physical organic chemistry concerned with fundamental aspects of chemical reactions and synthesis and the production of organic compounds.
Inhaltsverzeichnis zu „Flash Chemistry “
1. Introduction1.1 Flask chemistry
1.2 Flash chemistry
1.3 Flask chemistry or flash chemistry
2. The Background to Flash Chemistry
2.1 How do chemical reactions take place?
3. What is Flash Chemistry?
4. Why is Flash Chemistry Needed?
4.1 Chemical reaction, an extremely fast process at molecular level
4.2 Rapid construction of chemical libraries
4.3 Rapid synthesis of radioactive PET probes
4.4 On-demand rapid synthesis in industry
4.5 Conclusions
5. Methods of Activating Molecules
5.1 Thermal activation of organic molecules
5.2 Photochemical activation
5.3 Electrochemical activation
5.4 Chemical activation
5.5 Accumulation of reactive species
5.6 Continuous generation of reactive species in a flow system
5.7 Interconversion between reactive species
5.8 Conclusions
6. Methods of Activating Molecules
6.1 Mixing
6.2 Temperature control
6.3 Residence time control
6.4 Conclusions
7. Microfluidic Devices and Microflow Systems
7.1 Brief history
7.2 Characteristic features of microflow systems
7.3 Microstructured fluidic devices
7.4 Conclusions
8. Applications of Flash Chemistry in Organic Synthesis
8.1 Highly exothermic reactions which are difficult to control in macrobatch reactors
8.2 Reactions in which a reactive intermediate easily decomposes in macrobatch reactors
8.3 Reactions the products of which easily decompose in macrobatch reactors
8.4 Reactions in which undesired byproducts are produced in the subsequent reactions in macrobatch reactors
8.5 Reactions that can be accelerated using microflow systems
8.6 Summary
9. Polymer Synthesis Based on Flash Chemistry
9.1 Introduction
9.2 Chain-growth polymerization and step-growth polymerization
9.3 Molecular weight and molecular-weight distribution
9.4 Cationic polymerization
9.5 Free-radical polymerization
9.6 Summary
10. Industrial Applications of Flash Chemistry
10.1 Synthesis
... mehr
of diarylethene as photochromic compound (micrometer size single reactor)
10.2 Synthesis of pharmaceutically interesting spiro lactone fragment of nueropeptide Y (Millimeter size single reactor)
10.3 Grignard Exchange Process (Internal numbering-up)
10.4 Radical Polymerization Process (Numbering-up)
10.5 Other examples of industrial applications of flash chemistry
10.6 Flash chemistry as a powerful way of sustainable chemical synthesis
11. Outlook of Flash Chemistry
10.2 Synthesis of pharmaceutically interesting spiro lactone fragment of nueropeptide Y (Millimeter size single reactor)
10.3 Grignard Exchange Process (Internal numbering-up)
10.4 Radical Polymerization Process (Numbering-up)
10.5 Other examples of industrial applications of flash chemistry
10.6 Flash chemistry as a powerful way of sustainable chemical synthesis
11. Outlook of Flash Chemistry
... weniger
Bibliographische Angaben
- Autor: Jun-Ichi Yoshida
- 2008, 1. Auflage, 272 Seiten, Maße: 23,7 cm, Gebunden, Englisch
- Verlag: Wiley & Sons
- ISBN-10: 0470035862
- ISBN-13: 9780470035863
- Erscheinungsdatum: 08.10.2008
Sprache:
Englisch
Pressezitat
The book provides a nice, self consistent overview of the motivation for flow chemistry, the basic principles of chemical reactions and organic synthesis, and an examination of the concepts of fluid flow, heat and mass transfer, and devices. ( JACS , August 2009) "I found the book very readable and would recommend it to anyone wishing to learn about the benefits of microreactor technology.... The author has structured the book well; the introductory chapters clearly establish the basic concepts of microreactor technology." ( Chemistry World , March 2009)
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