Pesticide Protocols
(Sprache: Englisch)
A comprehensive collection of robust methods for the detection of pesticide compounds or their metabolites useful in food, environmental, and biological monitoring, and in studies of exposure via food, water, air, and the skin or lungs. The readily...
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A comprehensive collection of robust methods for the detection of pesticide compounds or their metabolites useful in food, environmental, and biological monitoring, and in studies of exposure via food, water, air, and the skin or lungs. The readily reproducible methods range from gas and liquid chromatography coupled to mass spectrometry detection and other classic detectors, to capillary electrophoresis and immunochemical or radioimmunoassay methods. The authors have focused on extraction and cleanup procedures, in order to develop and optimize more fullyautomated and miniaturized methods, including solid-phase extraction, solid-phase microextraction, microwave-assisted extraction, and on-line tandem liquid chromatography (LC/LC) trace enrichment, among others. The protocols offer step-by-step laboratory instructions, an introduction outlining the principles behind the technique, lists of the necessary equipment and reagents, and tips on troubleshooting and avoiding known pitfalls.
Klappentext zu „Pesticide Protocols “
A comprehensive collection of robust methods for the detection of pesticide compounds or their metabolites useful in food, environmental, and biological monitoring, and in studies of exposure via food, water, air, and the skin or lungs. The readily reproducible methods range from gas and liquid chromatography coupled to mass spectrometry detection and other classic detectors, to capillary electrophoresis and immunochemical or radioimmunoassay methods. The authors have focused on extraction and cleanup procedures, in order to develop and optimize more fullyautomated and miniaturized methods, including solid-phase extraction, solid-phase microextraction, microwave-assisted extraction, and on-line tandem liquid chromatography (LC/LC) trace enrichment, among others. The protocols offer step-by-step laboratory instructions, an introduction outlining the principles behind the technique, lists of the necessary equipment and reagents, and tips on troubleshooting and avoiding known pitfalls. Recent advances in the analysis of pesticide residues in both environmental and food commodities hold out the possibility of analyzing many pesticides in one analytical run. In Pesticide Protocols, expert researchers-who have each perfected the techniques they write about-describe in step-by-step detail robust methods for the detection of pesticide compounds or their metabolites, techniques that are highly useful in food, environmental, and biological monitoring, and in studies of exposure via food, water, air, and the skin or lungs. The methods range from gas and liquid chromatography coupled to mass spectrometry detection and other classic detectors, to capillary electrophoresis and immunochemical or radioimmunoassay techniques. The authors apply these broad-ranging techniques to the analysis of several families of pesticides, to pesticide residues in vegetables, to pesticides in water and air, and to pesticide exposure. The authors have focused on extraction and cleanup procedures in
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order to develop and optimize more fully automated and miniaturized methods, including solid-phase extraction, solid-phase microextraction, microwave-assisted extraction, and on-line tandem liquid chromatography trace enrichment, among others. The protocols follow the successful Methods in Biotechnology series format, each offering step-by-step laboratory instructions, an introduction outlining the principles behind the technique, lists of the necessary equipment and reagents, and tips on troubleshooting and avoiding known pitfalls.
Comprehensive and versatile, Pesticide Protocols offers analysts powerful and highly practical tools for analyzing the presence of pesticides in complex matrices.
Comprehensive and versatile, Pesticide Protocols offers analysts powerful and highly practical tools for analyzing the presence of pesticides in complex matrices.
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Inhaltsverzeichnis zu „Pesticide Protocols “
Part I. Analytical Methodologies to Determine Pesticides and Metabolites in Human Fat Tissues and Body FluidsAnalysis of Endocrine Disruptor Pesticides in Adipose Tissue Using Gas Chromatography-Tandem Mass Spectrometry: Assessment of the Uncertainty of the MethodJosé L. Martínez Vidal, Antonia Garrido Frenich, Francisco J. Egea González, and Francisco J. Arrebola LiébanasDetermination of Pyrethroids in Blood Plasma and Pyrethroid/Pyrethrin Metabolites in Urine by Gas Chromatography-Mass Spectrometry and High-Resolution GC-MSGabriele Leng and Wolfgang GriesA Multianalyte Method for the Quantification of Current-Use Pesticides in Human Serum or Plasma Using Isotope Dilution Gas Chromatography-High-Resolution Mass SpectrometryDana B. Barr, Roberto Bravo, John R. Barr, and Larry L. NeedhamApplication of Solid-Phase Disk Extraction Combined With Gas Chromatographic Techniques for Determination of Organochlorine Pesticides in Human Body FluidsAdrian CovaciA Comprehensive Approach for Biological Monitoring of Pesticides in Urine Using HPLC-MS/MS and GC-MS/MSDana B. Barr, Anders O. Olsson, Roberto Bravo, and Larry L. NeedhamUrinary Ethylenethiourea as a Biomarker of Exposure to EthylenebisdithiocarbamatesSilvia Fustinoni, Laura Campo, Sarah Birindelli, and Claudio ColosioAnalysis of 2,4-Dichlorophenoxyacetic Acid and 2-Methyl-4- Chloro-Phenoxyacetic Acid in Human UrineCristina Aprea, Gianfranco Sciarra, Nanda Bozzi, and Liana LunghiniDetermination of Herbicides in Human Urine by Liquid Chromatography-Mass Spectrometry With Electrospray IonizationIsabel C. S. F. Jardim, Joseane M. Pozzebon, and Sonia C. N. QueirozAnalysis of Pentachlorophenol and Other Chlorinated Phenols in Biological Samples by Gas Chromatography or Liquid Chromatography-Mass SpectrometryJi Y. ZhangAnalysis of 2,4-Dichlorophenoxyacetic Acid in Body Fluids of Exposed Subjects Using RadioimmunoassayDietmar KnoppA High-Throughput Screening Immunochemical Protocol for Biological Exposure Assessment of
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Chlorophenols in Urine SamplesMikaela Nichkova and M.-Pilar MarcoPart II. Assessment of Inhalatory and Potential Dermal ExposureAssessment of Postapplication Exposure to Pesticides in AgricultureJoop J. van Hemmen, Katinka E. van der Jagt, and Derk H. BrouwerField Study Methods for the Determination of Bystander Exposure to PesticidesC. Richard GlassDetermination of Household Insecticides in Indoor Air by Gas Chromatography-Mass SpectrometryEdith Berger-Preiss and Lutz ElfleinAssessment of Dermal and Inhalatory Exposure of Agricultural Workers to Malathion Using Gas Chromatography-Tandem Mass SpectrometryFrancisco J. Egea González, Francisco J. Arrebola Liébanas, and A. MarínPesticides in Human Fat and Serum Samples vs Total Effective Xenoestrogen BurdenPatricia Araque, Ana M. Soto, M. Fátima Olea-Serrano, Carlos Sonnenschein, and Nicolas OleaPart III. Pesticide Analysis in FoodQuality Criteria in Pesticide AnalysisAntonia Garrido Frenich, José L. Martínez Vidal, Francisco J. Egea González, and Francisco J. Arrebola LiébanasImmunoassay Methods for Measuring Atrazine and 3,5,6-Trichloro-2-Pyridinol in FoodsJeanette M. Van Emon and Jane C. ChuangQuick, Easy, Cheap, Effective, Rugged, and Safe Approach for Determining Pesticide ResiduesSteven J. LehotayDetermination of Organophosphorus Pesticide Residues in Vegetable Oils by Single-Step Multicartridge Extraction and Cleanup and by Gas Chromatography With Flame Photometric DetectorAlfonso Di Muccio, Anna M. Cicero, Antonella Ausili, and Stefano Di MuccioMulticlass Pesticide Analysis in Vegetables Using Low-Pressure Gas Chromatography Linked to Tandem Mass SpectrometryFrancisco J. Arrebola Liébanas, Francisco J. Egea González, and Manuel J. González RodríguezUse of Matrix Solid-Phase Dispersion for Determining Pesticides in Fish and FoodsSteven A. BarkerAnalysis of Fungicides in Fruits and Vegetables by Capillary Electrophoresis-Mass SpectrometryYolanda PicóApplication of Supercritical Fluid Extraction for the Analysis of Organophosphorus Pesticide Residues in Grain and Dried FoodstuffsKevin N. T. Norman and Sean H. W. PantonApplication of Microwave-Assisted Extraction for the Analysis of Dithiocarbamates in Food MatricesEuphemia Papadopoulou-Mourkidou, Emmanuil Nikolaos Papadakis, and Zisis VryzasEnantioselective Determination of a-Hexachlorocyclohexane in Food Samples by GC-MSChia-Swee Hong and Shaogang ChuPart IV. Pesticide Analysis in WaterAutomated Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry for Screening and Determination of Multiclass Pesticides in WaterTaizou Tsutsumi, Mitsushi Sakamoto, Hiroyuki Kataoka, and Janusz PawliszynAnalysis of Herbicides in Water by On-Line In-Tube Solid-Phase Microextraction Coupled With Liquid Chromatography-Mass SpectrometryHiroyuki Kataoka, Kurie Mitani, and Masahiko TakinoCoupled-Column Liquid Chromatography for the Determination of Pesticide ResiduesElbert Hogendoorn and Ellen DijkmanOn-Line Admicelle-Based Solid-Phase Extraction-Liquid Chromatography-Ionization Trap Mass Spectrometry for the Analysis of Quaternary Ammonium Herbicides in Drinking WaterDolores Pérez-Bendito, Soledad Rubio, and Francisco MerinoMolecular Imprinted Solid-Phase Extraction for Cleanup of Chlorinated Phenoxyacids From Aqueous SamplesClaudio Baggiani and Cristina GiovannoliAutomated Trace Analysis of Pesticides in WaterEuphemia Papadopoulou-Mourkidou, John Patsias, and Anna KoukourikouGas Chromatography-High-Resolution Mass Spectrometry-Based Method for the Simultaneous Determination of Organotin Compounds in WaterMichael G. Ikonomou and Marc P. FernandezDetermination of Triazine Herbicides and Degradation Products in Water by Solid-Phase Extraction and Chromatographic Techniques Coupled With Mass SpectrometryHassan Sabik and Roger JeannotAn Optical Immunosensor for Pesticide Determination in Natural WatersSara Rodríguez-Mozaz, Maria J. López de Alda, and Damia BarcelóIndex
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Bibliographische Angaben
- Autor: Jose L. Martinez Vidal
- 2005, 504 Seiten, Maße: 15,6 x 23,4 cm, Gebunden, Englisch
- Herausgegeben:Martínez Vidal, José L.
- Herausgegeben: Jos L. Martnez Vidal, Josa(c) L. Marta-Nez Vidal
- Verlag: Humana Press
- ISBN-10: 1588294102
- ISBN-13: 9781588294104
Sprache:
Englisch
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